Publication Type
Peer Reviewed Journal
Mandatory Citation Fields
Hollinger, M,Abraha, F,Oscarson, S;
2011
January
Carbohydrate Research
Synthesis of mucin O-glycan core structures as their p-nitro- and p-aminophenyl glycosides
Published
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Mucin O-glycan core structures Oxazolidinone protected glycosyl donors Oligosaccharide synthesis GLYCOSYLATION GLUCOSAMINE CARBOHYDRATE ANALOGS GLCNAC DONORS ACID
346
1454
1466
For the investigation of glycosidases, and for the construction of glycan arrays the p-nitrophenyl- and p-aminophenyl glycosides of mucin O-glycan core structures 1-7 and the 2,6-ST-antigen have been chemically synthesized using D-galactose as a precursor for GalNAc residues. GlcNAc residues have partly been introduced using a 4,6-di-O-benzoyl-2,3-N,O-oxazolidinone-protected donor, which allowed deprotection of the formed di- and tri-saccharides in one step using sodium methoxide. (C) 2011 Elsevier Ltd. All rights reserved.
DOI 10.1016/j.carres.2011.03.036
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