Publication Type
Publication Type
Peer Reviewed Journal
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Authors
Kamalraj V. Rajendran and Declan G. Gilheany
Year
2012
Month
February
Journal
Chemical Communications
Title
Simple unprecedented conversion of phosphine oxides and sulfides to phosphine boranes using sodium borohydride
Status
Published
Times Cited
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Volume
48
Issue
Start Page
817
End Page
819
Abstract
A variety of
phosphine oxides
and
sulfides
can be efficiently converted directly to the corresponding
phosphine
boranes
using
oxalyl chloride
followed by
sodium borohydride
. Optically active
P
-stereogenic
phosphine oxides
can be converted stereospecifically to
phosphine
boranes
with inversion of configuration by treatment with Meerwein's salt followed by
sodium borohydride
.
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